Royal Society of Chemistry

Palladium(II)-1-phenylthio-2-arylchalcogenoethane complexes: palladium phosphide nano-peanut and ribbon formation controlled by chalcogen and Suzuki coupling activation

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03471F, PaperAjai kumar Singh, Gyandshwar Kumar Rao, Arun Kumar, Fariha Saleem, Mahabir Pratap Singh, Satyendra Kumar, Bharat Kumar, Goutam Mukherjee
The ligands PhSCH2CH2EAr (L1-L3; E = S, Se or Te) and their Pd-complexes [PdLCl2]; (1-3] have been synthesized and authenticated with their 1H, 13C{1H}, 77Se{1H} and 125Te{1H} NMR spectra. Single...
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Nitrogen Enriched Mesoporous Organic Polymer Anchored Copper(II) Material: an Efficient and Reusable Catalyst for the Synthesis of Esters and Amides From aromatic systems

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03838J, PaperRostam Ali Molla, Md. Asif Iqubal, Kajari Ghosh, Kamaluddin Kamal, SM Islam
A new copper-grafted mesoporous poly-melamine-formaldehyde (Cu-mPMF) has been synthesized from melamine and paraformaldehyde in DMSO medium, followed by grafting of Cu(II) at its surface. Cu-mPMF has been characterized by elemental...
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Cyclic tetramers of five-membered palladacycle based on head-to-tail-linked isocyanate dimer and their reactivity in cyclotrimerization of isocyanates

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00534E, PaperYong-Joo Kim, Seon Gye Lee, Keun-Young Choi, SuJin Park, Soonwon Lee
Novel macrocyclic complexes, tetramers of a five-membered ring consisting of an organic isocyanate dimer and palladium, were prepared from bis(phosphine)palladium-styrene and benzyl isocyanate. Isocyanate cyclotrimerization with tetrameric or single palladacycles...
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Copper-Incorporated Mono- and Di-TeRu5 Metal Carbonyl Complexes: Syntheses, Structures, and an Unusual Skeletal Arrangement

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00546A, PaperMinghuey Shieh, Chia-Yeh Miu, Kai-Jieah Hsing, Li-Fing Jang, Chien-Nan Lin
Two sandwich-type Cu3Cl- or Cu2{Te2Ru4(CO)10}-bridging di-TeRu5 clusters, [{TeRu5(CO)14}2Cu3Cl]2─ (1) and [{TeRu5(CO)14}2Cu2{Te2Ru4(CO)10}]4─ (2), were obtained from the reaction of [TeRu5(CO)14]2─ with 1 equiv of [Cu(MeCN)4][BF4] in CH2Cl2 or THF at 0...
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Solvent-free synthesis of new inorganic-organic hybrid solids with finely tuned manganese oxalate structures

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00431D, CommunicationLindong Luan, Jing Li, Changzhen Yin, Zhien Lin, hui huang
Three manganese phosphate-oxalates have been synthesized under solvent-free conditions. These inorganic-organic hybrid solids are based on a pcu-type topology with nanobelt-like, sql-, and cds-type manganese oxalate skeletons, respectively. The amine...
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Synthesis of Cyclic Polyesters: Effects of Alkoxy Side Chain in Salicylaldiminato Tin(II) Complexes

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00139K, PaperPhonpimon Wongmahasirikun, Paweenuch Prom-on, Preeyanuch Sangtrirutnugul, Palangpon Kongsaeree, Khamphee Phomphrai
A new class of salicylaldiminato tin(II) catalysts having different alkoxy side chains has been developed. The ligands were modified to have different length and flexibility as -(CH2)2- (2a), -(CH2)3- (2b),...
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Solvent Effect on the Structures and Magnetic Properties of Two Doubly Interpenetrated Metal-Organic Frameworks

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT04006F, PaperFu-Ping Huang, Cheng Yang, Hai-Ye Li, Peng-Fei Yao, Xiao-Huan Qin, Shi-Ping Yan, Mohamedally Kurmoo
Two doubly interpenetrated coordination polymers [Co2(BDC)2(bpt)2].nSolvent based on dimeric secondary building units and crystallizing with distinct solvent molecules (1-H2O and 2-MeOH for nSolvent = 2H2O and MeOH.H2O, respectively), were obtained...
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In-situ characterization of uranium and americium oxide solid solution formation for CRMP process: first combination of in-situ XRD and XANES measurements

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03515A, PaperMarie Caisso, Sebastien Picart, renaud c belin, Florent LEBRETON, Philippe Martin, Kathy Dardenne, Joerg Rothe, Daniel R. Neuville, THIBAUD DELAHAYE, Andre Ayral
Transmutation of americium in heterogeneous mode through the use of U1-xAmxO2+/-[small delta] ceramic pellets, also known as Americium Bearing Blankets (AmBB), has become a major research axis. Nevertheless, in order to...
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Stepwise assembly of a semiconducting coordination polymer [Cd8S(SPh)14(DMF)(bpy)]n and its photodegradation of organic dyes

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03687E, PaperChao Xu, Niklas Hedin, Hua-Tian Shi, Zhifeng Xin, Qian-Feng Zhang
Chalcogenolate clusters can be interlinked with organic linkers into semiconducting coordination polymers with photocatalytic properties. Here, discrete clusters of Cd8S(SPh)14(DMF)3 were interlinked with 4,4'-bipyridine into a one dimensional coordination polymer...
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An open chain carboxyethyltin functionalized sandwich-type tungstophosphate based on trivacant Dawson subunit: synthesis, characterization and properties

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00361J, Paperjianping Bai, fang Su, Hao-Tian Zhu, hang Sun, Lan-Cui Zhang, Meiying Liu, wansheng You, Zaiming Zhu
A Dawson sandwich-type polyoxometalate {C(NH2)3}12H4[[small alpha][small beta][small beta][small alpha]-{(Sn(C3H4O2))2Mn2(P2W15O56)2}][round bullet, filled]22H2O (Abbreviated as SnR-Mn-P2W15), functionalized by open chain carboxyethyltin groups was first prepared in aqueous solution under conventional reaction conditions, and structurally characterized by physico-chemical and...
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Novel metal-organic framework with tunable fluorescence property: supramolecular signaling platform for polynitrophenolics

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00489F, CommunicationRik Rani Koner, Mangili Venkateswarulu, Avijit Pramanik
With the aid of a rotational C3-symmetric tricarboxytriphenylamine based ligand, a new Cd-MOF was synthesized and characterized by various spectroscopic techniques as well as by single-crystal X-ray diffraction analysis. The...
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An electrochemical aptasensor based on TiO2/three-dimensional reduced graphene oxide/PPy nanocomposite for the sensitive detection of lysozyme

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00168D, PaperMinghua Wang, Shuyong Zhai, Zihan Ye, Linghao He, Donglai Peng, Xiaozhong Feng, Yanqin Yang, shaoming fang, Hongzhong Zhang, Zhihong Zhang
A sensitive aptasensor based on a nanocomposite of hollow titanium dioxide nanoball, three-dimensional reduced graphene oxide, and polypyrrole (TiO2/3D-rGO/PPy) was developed for lysozyme detection. Lysozyme aptamer was easily immobilized onto...
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Synthesis, Structure, and Magnetic Properties of Novel B-site Ordered Double Perovskites, SrLaMReO6 (M = Mg, Mn, Co and Ni)

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03821E, PaperJohn E Greedan, Corey M. Thompson, Lisheng Chi, Alannah Hallas, Murray Wilson, Timothy Munsie, Ian Swainson, Andrew Paul Grosvenor, John R Hayes, Graeme Luke
This is an Accepted Manuscript, which has been through the RSC Publishing peer review process and has been accepted for publication. Accepted manuscripts are published online shortly after acceptance. This version of the article will be replaced by the fully edited, formatted and proof read Advance Article as soon as this is available.
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Ethylene polymerization by the thermally unique 1-[2-(bis(4-fluorophenyl)methyl)-4,6-dimethylphenylimino]-2-aryliminoacenaphthylnickel precursors

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00052A, PaperShizhen Du, Qifeng Xing, Zygmunt Flisak, Erlin Yue, Yang Sun, Wen Hua Sun
This is an Accepted Manuscript, which has been through the RSC Publishing peer review process and has been accepted for publication. Accepted manuscripts are published online shortly after acceptance. This version of the article will be replaced by the fully edited, formatted and proof read Advance Article as soon as this is available.
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Location of Ge and extra-framework species in the zeolite ITQ-24

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT03831B, PaperAna Belen Pinar, L McCusker, Christian Barlocher, Sonjong Hwang, Joel Schmidt, Mark E. Davis, Stacey Zones
The germanosilicate ITQ-24 (IWR framework type) was synthesized in fluoride medium using 1,3,5-tris(1,2-dimethylimidazolium) benzene as the structure directing agent (SDA). A structure analysis of the as-synthesized ITQ-24 material using synchrotron...
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Charge transfer salts of BEDT-TTF with lithium tris(oxalato)metallate(III)

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00183H, PaperLee Martin, Hendrik Engelkamp, Hiroki Akutsu, Shinichi Nakatsuji, Jun-ichi Yamada, Peter Horton, M Hursthouse
The first radical cation salts in the extensive family (BEDT-TTF)x[(A)M(C2O4)3].Guest containing lithium as the counter cation have been synthesized and characterised.
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New NIR-emissive tetranuclear Er(III) complexes with 4-hydroxo-2,1,3-benzothiadiazolate and dibenzoylmethanide ligands: synthesis and characterization

Dalton Transactions - 3 March, 2015 - 06:17

Dalton Trans., 2015, Advance Article
DOI: 10.1039/C4DT03878A, PaperTaisiya S. Sukhikh, Denis A. Bashirov, Natalia V. Kuratieva, Anton I. Smolentsev, Artem S. Bogomyakov, Vladimir A. Burilov, Asia R. Mustafina, Andrey V. Zibarev, Sergey N. Konchenko
Two new Er complexes were prepared and studied.
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3+1)-Dimensional commensurately modulated structure and photoluminescence properties of diborate KSbOB2O5

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C5DT00267B, PaperDan Zhao, Rong-Hua Zhang, Fei-Fei Li, Juan Yang, Bing-Guo Liu, Yun-Chang Fan
ingle-crystal of diborate KSbOB2O5 has been prepared under high temperature molten-salt method and its structure has been determined by single crystal X-ray diffraction analysis. Diffraction pattern show strong main reflections...
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A Stable Phosphanyl Phosphaketene and Its Reactivity

Dalton Transactions - 3 March, 2015 - 06:17
Dalton Trans., 2015, Accepted Manuscript
DOI: 10.1039/C4DT04012K, PaperH Grutzmacher, Zhongshu Li, Chengyong Su, Xiaodan Chen, Maike Bergeler, Markus Reiher
Sodium phospaethynolate, Na(OCP), reacts with the bulky P-chloro-diazaphosphole yielding a phosphanyl phosphaketene, which is stable for weeks under inert atmosphere in the solid state. This compound is best described as...
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Synthesis of sulfonamide conjugates of Cu(II), Ga(III), In(III), Re(V) and Zn(II) complexes: carbonic anhydrase inhibition studies and cellular imaging investigations

Dalton Transactions - 3 March, 2015 - 06:17

Dalton Trans., 2015, Advance Article
DOI: 10.1039/C4DT03206C, PaperJonathan R. Dilworth, Sofia I. Pascu, Philip A. Waghorn, Daniela Vullo, Simon R. Bayly, Martin Christlieb, Xin Sun, Claudiu T. Supuran
New sulfonamides and their metal complexes are reported, with a focus on porphyrin derivatives for simultaneous cellular optical imaging, radiolabelling and Carbonic Anhydrase inhibition capabilities.
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